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Iron 57 Fe (2.19%, I = 1/2) is the only NMR-active isotope, The 57 Fe nucleus is one of the most insensitive nuclei in NMR spectroscopy. Its low natural abundance and nuclear magnetic properties are not favourable for direct detection of 57 Fe NMR signals and observation of indirect nuclear 57 Fe-X spin-spin couplings.

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Utilizing the technique of probe layers, i.e., inserting 57 Fe in various depths of the thin film (see Fig. 8), NRS directly probes the actual spin structure in various depths by selectively exciting the 57 Fe layer at various lateral positions (Röhlsberger et al. 2002).